HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 23445077, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 69043488 | HCID 69043488 | — |
| Product | HCID 23445077 | HCID 23445077 | — |
Reaction Steps
Following the general method described in example 388, 1-quinolin-8-yl-1H-imidazole-4-carboxylic acid ethyl ester was reacted with diisobutylaluminum hydride. After hydrolytic workup and chromatography the title compound was obtained as a light brown crystalline solid. Mp. 168-170° C. (Et2O), MS: m/e=225 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06610723B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-1ec2678aa3e346ebba4f34f569d32f08 |
| Source note | uspto-grants-2003_08 |