2-Morpholinoethylamine → HCID 70020870, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of Intermediate 4 (0.034 g, 0.062 mmol), 4-(2-aminoethyl)morpholine (0.041 ml, 0.31 mmol) and DMSO (0.03 ml); in a sealed vial (e.g. Reacti-vial™) was heated at 80° C. for 28 h. Purification by Autoprep. HPLC afforded the title compound after freeze drying as a white solid (0.015 g). LC/MS system A Rt=3.67 mins, m/z=642MH+

Provenance & Evidence