Octadecyl isocyanate → HCID 18183860, compound

Participants

Reaction Steps

10.1 Grams of N-hydroxyethylpyrrolidine, 23.6 g of octadecyl isocyanate and 100 ml of acetone were charged in a flask equipped with a stirrer and a condenser and refluxed with heating for 3 hours under stirring. The reaction mixture was cooled to room temperature, and the precipitated crystal was filtered off under reduced pressure and washed with acetone, followed by recrystallization from n-hexane to obtained 18.5 g of the desired product. m.p. 57° C.

Provenance & Evidence