HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 53986334, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ethyl 2-chloro-3-(2-chloro-5-(1,3-dioxo-1,3,4,5,6,7-hexahydro-2H-isoindol-2-yl)phenyl)-2-propenoate | HCID 3525006 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 53986334 | HCID 53986334 | — |
Reaction Steps
Ammonia gas was passed into a solution of 5.9 g of N-[4-chloro-3-(2-chloro-2-ethoxycarbonylethenyl)-phenyl]-3,4,5,6-tetrahydrophthalimide in 150 ml of acetonitrile until saturation was reached. The reaction mixture obtained was then stirred for a further 19 hours at 20°-25° C., after which the solid formed was separated off and then washed with petroleum ether. Mp.: 185°-186° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05817603 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-18a9c018956e4bc493d4230da42790e8 |
| Source note | uspto-grants-1998_10 |