HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-2-thenoyl Chloride → HCID 19601507, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-2-thenoyl Chloride | HCID 2737605 | — |
| Reactant | 3-(1-Methyl-piperidin-4-yl)-1H-pyrrolo[3,2-b]pyridin-5-ylamine | HCID 10220230 | — |
| Product | HCID 19601507 | HCID 19601507 | 83% |
Reaction Steps
Beginning with 0.40 gm (1.74 mMol) 5-amino-3-(1-methylpiperidin-4-yl)pyrrolo[3,2-b]pyridine and 0.34 gm (2.08 mMol) 3-methyl-2-thiophenecarbonyl chloride, 0.51 gm (83%) of the title compound were prepared as a light brown foam essentially by the procedure described in Example 4. A sample was crystallized from ethanol/water for analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05817671 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-ec90a36035eb4b7382cb3d97afb62edc |
| Source note | uspto-grants-1998_10 |