Water → HCID 18969592, compound

Participants

Reaction Steps

A solution of 2-(p-chlorophenyl)-3-(phenylthio)pyrrole (1.0 g, 3.5 mmol) in methanol is treated with a solution of potassium peroxymonosulfate (2.95 g) in water (7.6 mL), stirred at room temperature for 5 hours, diluted with additional methanol, treated with a solution of potassium peroxymonosulfate (2.5 g) in water (7.4 mL), stirred at room temperature overnight and filtered to obtain a solid which is washed with water and dried to give the title product as a solid (mp 158°-159° C.).

Provenance & Evidence