HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 399078Generated: October 25, 2026
Triphenylphosphine → 4-Methylthiobenzyltriphenylphosphonium chloride
https://huagongshe.com/reaction/399078
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 1-(Chloromethyl)-4-(methylthio)benzene | HCID 70128 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 4-Methylthiobenzyltriphenylphosphonium chloride | HCID 18969794 | — |
Reaction Steps
A solution of 4-methylthiobenzyl chloride (3.1 g) and triphenylphosphine (4.72 g) was heated in toluene (35 mL) at reflux for 18 hr. The mixture was cooled to 0° C. and filtered. The resulting solid was used as such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05817700 |
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| Source dataset | uspto-grants-1998_10 |
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| ORD ID | ord-465b6066befc43b98bac8ccf3782c5b8 |
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| Source note | uspto-grants-1998_10 |
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