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HRID399079

反应详情

EQUATION

反应方程式

HRID 399079 的结构方程式

REACTANTS

反应物

1
结构：CSc1ccc(C[P+](c2ccccc2)(c2ccccc2)c2ccccc2)cc1.[Cl-]
HCID18969794

{[4-(Methylsulfanyl)phenyl]methyl}(triphenyl)phosphanium chloride

C26H24ClPS

PRODUCTS

生成物

1
结构：CSc1ccc(/C=C/c2ccc(SC)cc2)cc1
HCID12652959

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Cl-].c1ccc(C[P+](c2ccccc2)(c2ccccc2)c2ccccc2)cc1
催化剂HCID70671

Benzyltriphenylphosphonium chloride

C25H22ClP

PROCEDURE

实验过程

Following the procedure as describe in method 1, but sustituting 4-methylthiobenzyltriphenylphosphonium chloride for benzyltriphenylphosphonium chloride, the desired residue was purified by flash chromatography (silica gel; hexane/EtOAc (90:10)) and recrystallisation from hexane.

WORKUP

后处理

  1. customthe desired residue was purified by flash chromatography (silica gel; hexane/EtOAc (90:10)) and recrystallisation from hexane