HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-((5-Methoxy-1H-indol-6-yl)oxy)-N,N-dimethylethan-1-amine → 1-(4'-Acetyl-3'-methylbiphenyl-4-carbonyl)-6-(2-dimethylaminoethoxy)-5-methoxy-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-((5-Methoxy-1H-indol-6-yl)oxy)-N,N-dimethylethan-1-amine | HCID 10537659 | — |
| Reactant | 4'-Acetyl-3'-methylbiphenyl-4-carboxylic acid | HCID 18970493 | — |
| Product | 1-(4'-Acetyl-3'-methylbiphenyl-4-carbonyl)-6-(2-dimethylaminoethoxy)-5-methoxy-1H-indole | HCID 18970489 | — |
Reaction Steps
The title compound was prepared from 4'-acetyl-3'-methylbiphenyl-4-carboxylic acid (D21) and 6-(2-dimethylaminoethoxy)-5-methoxy-1H-indole (D13) using a similar procedure to Example 4 as an off-white solid mp 125°-127° C. (36%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05817833 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-d0c3a23c900647568b2db0dfb1fc4fdc |
| Source note | uspto-grants-1998_10 |