참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,3-Cyclopentadiene, 5-(1-methylethylidene)- | HCID 137467 | — |
| 반응물 | Potassium, (diphenylmethyl)- | HCID 11858962 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | HCID 131720872 | HCID 131720872 | — |
반응 단계
Potassium diphenylmethanide (5.72 g, 27.8 mmols) in about 50 mL of THF was slowly added to 6,6-dimethylfulvene (2.94 g, 27.8 mmols) in about 100 mL of THF at about 25 C. The reaction mixture was stirred at about 25° C. for about 16 hours. The solvent was removed under reduced pressure to give the desired product as a sticky, oily solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05817849 |
|---|
| 출처 데이터셋 | uspto-grants-1998_10 |
|---|
| ORD ID | ord-977dbb3c7fbe44209e362dc473b9d505 |
|---|
| 출처 메모 | uspto-grants-1998_10 |
|---|
