HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-nitrobenzoic acid → Benzoyl chloride, 2-chloro-4-nitro-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-nitrobenzoic acid | HCID 7448 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Product | Benzoyl chloride, 2-chloro-4-nitro- | HCID 81522 | — |
Reaction Steps
A mixture of 2-chloro-4-nitrobenzoic acid (20 g), thionyl chloride (40 ml) and DMF (5 drops) was stirred and heated to reflux for 1 hour. The mixture was evaporated to give 2-chloro-4-nitrobenzoyl chloride which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05821246 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-88cfdce930984ced9680cc96ebee8d71 |
| Source note | uspto-grants-1998_10 |