Dimethylamine → N,N-Dimethyl-1,4-dioxaspiro[4.5]decan-8-amine

HRID 399557Notes

Reaction equation

HRID 399557 reaction equation
[O:1]1[C:5]2([CH2:10][CH2:9][C:8](=O)[CH2:7][CH2:6]2)[O:4][CH2:3][CH2:2]1.[CH3:12][NH:13][CH3:14]>CO>[CH3:12][N:13]([CH3:14])[CH:8]1[CH2:9][CH2:10][C:5]2([O:4][CH2:3][CH2:2][O:1]2)[CH2:6][CH2:7]1

Participants

4

Reactant 2

HCID 674DimethylamineHCID 5674151,4-Dioxaspiro[4.5]decan-8-one

Product 1

HCID 361167N,N-Dimethyl-1,4-dioxaspiro[4.5]decan-8-amine

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Prepared from 1,4-dioxaspiro[4.5]decan-8-one and dimethylamine. Pale brown oil, Rf : 0.28 (silica gel; methylene chloroide/methanol/concentrated ammonia=9:1:0.1)

Sources & evidence

ORD record
ord-fe40f8fa4ab74118a3dd94fcac4bfd9c
Source dataset
uspto-grants-1998_10
Patent number
US05821240

Reaction notes

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