HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18943645, compound → HCID 18943673, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18943645 | HCID 18943645 | — |
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18943673 | HCID 18943673 | — |
Reaction Steps
Prepared from 1-(4-benzyloxyphenyl)-3-[2-(ethoxycarbonyl)ethyl]-3H-imidazol-2-one by hydrogenation in the presence of palladium on charcoal in ethanol at 40° C. and a hydrogen pressure of 50 psi. Rf value: 0.20 (silica gel; methylene chloride/methanol=100:2)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05827849 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-43c980414b954d0d994e3b53f440a66c |
| Source note | uspto-grants-1998_10 |