HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl formate → 2-hydroxy-3-ethoxycarbonyl-7-benzyl-6,7,8,9-tetrahydro-5H-pyrido[2,3-d]azepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl formate | HCID 8025 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Ethyl 2-carbamoylacetate | HCID 238112 | — |
| Reactant | 1-Benzyl-hexahydro-4H-azepin-4-one | HCID 1514350 | — |
| Product | 2-hydroxy-3-ethoxycarbonyl-7-benzyl-6,7,8,9-tetrahydro-5H-pyrido[2,3-d]azepine | HCID 178468541 | — |
Reaction Steps
Prepared from 1-benzyl-hexahydro-4-azepinone with ethyl formate and ethyl malonamate in the presence of sodium hydride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05827849 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-973610efe5e94a6cbb2e86d21018b0ac |
| Source note | uspto-grants-1998_10 |