HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 5-bromovalerate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 5-Bromovaleric acid | HCID 16368 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Ethyl 5-bromovalerate | HCID 84580 | — |
Reaction Steps
A! Starting from 5-bromopentanoic acid (50 g, 0.276 mole) and thionyl chloride (39 ml, 0.552 mole) in absolute ethanol (500 ml) and following the procedure of Example 13,A!, there were obtained 62.7 g of ethyl 5-bromopentanoate (quantitative yield) which was used as such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05827881 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-fb8a0eb019d5437d82002e139ae4bcb3 |
| Source note | uspto-grants-1998_10 |