HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → Methyl 3-(3-bromophenyl)prop-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 3-(3-Bromophenyl)acrylic acid | HCID 36251 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 3-(3-bromophenyl)prop-2-enoate | HCID 610698 | — |
Reaction Steps
To a solution of 50.0 g (220 mmol, Aldrich) of 3-bromocinnamic acid in 1 L sieve-dried methanol (Burdick & Jackson), stirred at 0° C., was added dropwise a solution of acidic methanol (prepared by the addition of 2.5 mL acetyl chloride to 250 mL methanol). The reaction
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05827868 |
| Source dataset | uspto-grants-1998_10 |
| ORD ID | ord-f8d184a5c3014a92bc4fb77c554723dc |
| Source note | uspto-grants-1998_10 |