9-Decen-1-ol → HCID 10526177, compound

HRID 400347Notes

Reaction equation

HRID 400347 reaction equation
[C:1](Cl)(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[CH2:21](O)[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH:29]=[CH2:30].C(OCC)(=[O:34])C.CCCCCC>>[C:1]([O:19][CH2:30][CH2:29][CH2:28][CH2:27][CH2:26][CH2:25][CH2:24][CH2:23][CH:22]=[CH2:21])(=[O:34])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

4

Reactant 3

HCID 256129-Decen-1-olHCID 5364783Oleoyl chlorideHCID 21226206Ethyl acetate hexane

Product 1

HCID 10526177HCID 10526177, compoundYield 97.5%

Procedure

Compound F was prepared from Oleoyl chloride and 9-decen-1-ol following the general procedure already discussed and shown in FIG. 11. Pure compound F was a colorless oil obtained by column chromatography with Ethyl acetate/Hexane=1:40.

Sources & evidence

ORD record
ord-74aa5e5576d7455fa7be6743a8818c9c
Source dataset
uspto-grants-2014_06
Patent number
US08741822B2

Reaction notes

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