HRID400423

反应详情

EQUATION

反应方程式

HRID 400423 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

150 mg palladium charcoal was added to 765 mg 4-(6-methoxy-pyrimidin-4-yl)-3,6-dihydro-2H-pyridine-1-carboxylic acid tert-butyl ester in 90 mL methanol. The reaction was stirred 3.5 h at RT and 3 bar hydrogen. Then, the reaction was filtered and evaporated to give 769 mg of the desired product.

WORKUP

后处理

  1. filtrationThen, the reaction was filtered
  2. customevaporated