HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indole-5-carbonitrile → N'-hydroxy-1H-indole-5-carboximidamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indole-5-carbonitrile | HCID 27513 | — |
| Reactant | N'-hydroxy-3H-benzimidazole-5-carboximidamide | HCID 178513241 | — |
| Product | N'-hydroxy-1H-indole-5-carboximidamide | HCID 4387213 | — |
Reaction Steps
The title compound was prepared following procedure described for Intermediate 1, step 2, but starting from 5-cyanoindole (2 g; 14.07 mmol) as a brown solid (2.4 g, 97%). HPLC (Method A), Rt 0.95 min (Purity: 88.8%). LC/MS (Method B): 176.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08741923B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-d087c9965bff4f6890bac22d85eafc97 |
| Source note | uspto-grants-2014_06 |