HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2R)-2-(Methoxymethyl)pyrrolidine → HCID 71558050, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2R)-2-(Methoxymethyl)pyrrolidine | HCID 671216 | — |
| Reactant | 5-tert-Butyl-3-(2-chloro-benzyl)-7-morpholin-4-yl-3H-[1,2,3]triazolo[4,5-d]pyrimidine | HCID 1433953 | — |
| Reactant | 5-tert-butyl-7-chloro-3-(2-chlorobenzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine | HCID 86683284 | — |
| Product | HCID 71558050 | HCID 71558050 | — |
Reaction Steps
In analogy to the procedure described for the synthesis of 5-tert-butyl-3-(2-chloro-benzyl)-7-morpholin-4-yl-3H-[1,2,3]triazolo[4,5-d]pyrimidine (example 1, step c), the title compound was prepared from 5-tert-butyl-7-chloro-3-(2-chlorobenzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine and (R)-2-(methoxymethyl)pyrrolidine and isolated as colorless gum (12.4 mg, 64%). MS (m/e): 415.4 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08741906B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-992d1c1262cd4014bd52844e9bb97d71 |
| Source note | uspto-grants-2014_06 |