HRID400916

反应详情

EQUATION

反应方程式

HRID 400916 的结构方程式

PROCEDURE

实验过程

In analogy to the procedure described for the synthesis of 5-tert-butyl-7-(3,3-difluoropyrrolidin-1-yl)-3-ethyl-3H-[1,2,3]triazolo[4,5-d]pyrimidine (example 61), the title compound was prepared from 5-tert-butyl-7-(3,3-difluoropyrrolidin-1-yl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine and 2-bromo-1-(pyridin-2-yl)ethanone hydrobromide and isolated as dark-brown solid. MS (m/e): 402.3 (MH+).

WORKUP

后处理

  1. customisolated as dark-brown solid