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HRID400933

反应详情

EQUATION

反应方程式

HRID 400933 的结构方程式

REACTANTS

反应物

3
结构：COc1ccc(Cn2nnc3c(N4CCOCC4)nc(C(C)(C)C)nc32)cc1
HCID71558051

未命名化合物

结构：COc1ccc(Cn2nnc3c(Cl)nc(C(C)(C)C)nc32)cc1
HCID86683299

未命名化合物

结构：Cl.OC[C@@H]1NCC[C@@H]1O
HCID86683343

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(Cn2nnc3c(N4CC[C@H](O)[C@@H]4CO)nc(C(C)(C)C)nc32)cc1
HCID86683342

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described for the synthesis of 4-(5-tert-butyl-3-(4-methoxybenzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidin-7-yl)morpholine (example 58, step c), the title compound was prepared from 5-tert-butyl-7-chloro-3-(4-methoxybenzyl)-3H-[1,2,3]triazolo[4,5-d]pyrimidine and (2S,3S)-2-(hydroxymethyl)pyrrolidin-3-ol hydrochloride and isolated as light-yellow gum. MS (m/e): 413.4 (MH+).

WORKUP

后处理

  1. customisolated as light-yellow gum