HRID401443

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(C)(C)OC(=O)NCc1cc(NC(=O)c2c[nH]c3ccccc3c2=O)ccc1C(C)(C)C

HCID66674656

未命名化合物

PRODUCTS

生成物

结构：CC(C)(C)c1ccc(NC(=O)c2c[nH]c3ccccc3c2=O)cc1CN

HCID57567307

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

N-[3-(Aminomethyl)-4-tert-butyl-phenyl]-4-oxo-1H-quinoline-3-carboxamide (390) was synthesized following the general scheme above starting from [5-[(4-oxo-1H-quinolin-3-yl)carbonylamino]-2-tert-butyl-phenyl]methylaminoformic acid tert-butyl ester (465). HPLC ret. time 2.44 min, 10-99% CH3CN, 5 min gradient; ESI-MS m/z 350.3 (M+H)+.