HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxypyrimidine-5-boronic acid → HCID 86670608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxypyrimidine-5-boronic acid | HCID 2736778 | — |
| Reactant | 6-Bromoimidazo[1,2-a]pyridine-3-carbaldehyde | HCID 21345676 | — |
| Product | HCID 86670608 | HCID 86670608 | 55.55% |
Reaction Steps
The title compound was prepared by following the procedure as described for Intermediate 1 using 6-bromoimidazo[1,2-a]pyridine-3-carbaldehyde and 2-methoxypyrimidin-5-ylboronic acid. Yield: 55.55%; 1H NMR (DMSO-d6; 300 MHz): δ 10.01 (s, 1H), 9.62 (s, 1H), 9.00 (s, 2H), 8.59 (s, 1H), 8.04-8.05 (m, 2H), 3.99 (s, 3H); MS: m/z 254 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08741932B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-4e09c5bedea04900bb58e82f595310ba |
| Source note | uspto-grants-2014_06 |