HRID401609

反应详情

EQUATION

反应方程式

HRID 401609 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Furthermore, 7-benzyloxyindole (404 mg, 1.81 mmol) was hydrogenated over 10% palladium on carbon (40 mg) in EtOH (4.2 mL) at ambient temperature under atmosphere pressure for 6 h. The catalyst was filtered off and washed with EtOH. The filtrate was concentrated to give 7-hydroxyindole as pale purple crystals, which was rapidly and directly used for the next reaction.

WORKUP

后处理

  1. filtrationThe catalyst was filtered off
  2. washwashed with EtOH
  3. concentrationThe filtrate was concentrated