HCID 44539696, compound → HCID 44539698, compound

Participants

Reaction Steps

Product 22 was synthesized following a procedure similar to the one described above for the synthesis of 5-((4-fluorophenylamino)methyl)-N,3-dihydroxy-4-(hydroxymethyl)picolinamide starting from methyl 5-((4-fluorophenethylamino)methyl)-3-hydroxy-4-(hydroxymethyl)picolinate (compound 22b). 1H-NMR (500 MHz, DMSO-d6) δ ppm 8.08 (s, 1H), 7.24 (m, 2H), 7.09 (t, J=7.2 Hz, 2H), 4.58 (s, 2H), 3.92 (s, 2H), 2.80 (m, 2H), 2.76 (m, 2H). MS-ESI m/z 336 [MH]+

Provenance & Evidence