HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 44540662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 58360284 | HCID 58360284 | — |
| Product | HCID 44540662 | HCID 44540662 | — |
Reaction Steps
Methyl 5-((benzyl(4-fluorophenyl)amino)methyl)-2,2-dimethyl-4H-[1,3]dioxino[4,5-c]pyridine-8-carboxylate 25a was prepared from methyl 5-((4-fluorophenylamino)methyl)-2,2-dimethyl-4H-[1,3]dioxino[4,5-c]pyridine-8-carboxylate (21a) (120 mg, 0.3 mmol), benzaldehyde (100 uL, 1.0 mmol) and sodium cyanoborohydride (28 mg, 0.45 mmol) according to the procedure described in Example 24. MS-ESI m/z 437 [MH]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08742123B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-af8166d615f0412a88a69aac5d5b7a77 |
| Source note | uspto-grants-2014_06 |