HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178469515, compound → HCID 178516395, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178469515 | HCID 178469515 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178516395 | HCID 178516395 | 25.4% |
Reaction Steps
A solution of the compound (0.050 g, 0.13 mmol) of Example 1 in N,N-dimethylformamide (1.0 mL) was refluxed for 6 h. Cooled to ambient temperature, the reaction mixture was purified by preparative HPLC to afford the titled compound as solid (0.010 g, y. 25%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08742113B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-2ba57fdfa82d4ac9876607a642704aaf |
| Source note | uspto-grants-2014_06 |