HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178469534, compound → HCID 178516405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178469534 | HCID 178469534 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178516405 | HCID 178516405 | 23% |
Reaction Steps
A solution of the compound (0.040 g, 0.098 mmol) of Example 9 in N,N-dimethylformamide (1.0 mL) was refluxed for 6 h. Cooled to ambient temperature, the reaction mixture was purified by preparative HPLC to afford the titled compound as solid (0.0075 g, y. 23%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08742113B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-8a96a7bb1d6b4c328a7d191542e7acb9 |
| Source note | uspto-grants-2014_06 |