HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178469511, compound → HCID 178516391, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178469511 | HCID 178469511 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178516391 | HCID 178516391 | 12.3% |
Reaction Steps
A solution of the compound (0.050 g, 0.12 mmol) of Example 15 in N,N-dimethylformamide (1.0 mL) was stirred at 150° C. for 6 h. Cooled to ambient temperature, the reaction mixture was purified by preparative HPLC to afford the titled compound as solid (0.0050 g, y. 11%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08742113B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-20a69fe854a04f08848e66bc235948a1 |
| Source note | uspto-grants-2014_06 |