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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 402718Generated: October 31, 2026

HCID 178469589, compound → HCID 178492140, compound

https://huagongshe.com/reaction/402718

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178469589HCID 178469589—
SolventDimethylformamideHCID 6228—
ProductHCID 178492140HCID 17849214018%

Reaction Steps

A solution of the compound (0.10 g, 0.23 mmol) of Example 24 in N,N-dimethylformamide (3.0 mL) was refluxed for 7 h. Cooled to ambient temperature, the reaction mixture was purified by preparative HPLC to afford the titled compound as solid (0.015 g, y. 18%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08742113B2
Source datasetuspto-grants-2014_06
ORD IDord-773f7042662b4da488e87edf8455fbf0
Source noteuspto-grants-2014_06