HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178469589, compound → HCID 178492140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178469589 | HCID 178469589 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178492140 | HCID 178492140 | 18% |
Reaction Steps
A solution of the compound (0.10 g, 0.23 mmol) of Example 24 in N,N-dimethylformamide (3.0 mL) was refluxed for 7 h. Cooled to ambient temperature, the reaction mixture was purified by preparative HPLC to afford the titled compound as solid (0.015 g, y. 18%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08742113B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-773f7042662b4da488e87edf8455fbf0 |
| Source note | uspto-grants-2014_06 |