HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178469531, compound → HCID 178439206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178469531 | HCID 178469531 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178439206 | HCID 178439206 | — |
Reaction Steps
A solution of the compound (0.12 g, 0.29 mmol) of Example 37 in N,N-dimethylformamide (3.0 mL) was refluxed for 6 h. Cooled to ambient temperature, the reaction mixture was purified by preparative HPLC to afford 2-[(1H-pyrrolo[2,3-b]pyridin-3-yl)methylene]-5-[(4-isopropylphenyl)amino]furan-3(2H)-one as solid (0.0050 g, y. 5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08742113B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-6a82a086cd934455ae809da34755f42f |
| Source note | uspto-grants-2014_06 |