HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178469597, compound → HCID 178492139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178469597 | HCID 178469597 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178492139 | HCID 178492139 | 13.9% |
Reaction Steps
A solution of the compound (0.043 g, 0.099 mmol) of Example 28 in N,N-dimethylformamide (1.2 mL) was refluxed for 6 h. Cooled to ambient temperature, the reaction mixture was purified by preparative HPLC to afford the titled compound (0.0050 g, y. 12%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08742113B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-cbf54e7fe5604d0088785f7f0ae5603c |
| Source note | uspto-grants-2014_06 |