HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178469557, compound → HCID 178516424, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178469557 | HCID 178469557 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178516424 | HCID 178516424 | 4% |
Reaction Steps
A solution of the compound (0.099 g, 0.24 mmol) of Example 53 in N,N-dimethylformamide (1.0 mL) was refluxed for 4 h. Cooled to ambient temperature, the reaction mixture was purified by preparative HPLC to afford the titled compound as solid (0.0030 g, y. 4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08742113B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-5d311e557208471ebc544a6080e2ccf5 |
| Source note | uspto-grants-2014_06 |