Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 402723Generated: October 30, 2026

HCID 178469557, compound → HCID 178516424, compound

https://huagongshe.com/reaction/402723

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178469557HCID 178469557—
SolventDimethylformamideHCID 6228—
ProductHCID 178516424HCID 1785164244%

Reaction Steps

A solution of the compound (0.099 g, 0.24 mmol) of Example 53 in N,N-dimethylformamide (1.0 mL) was refluxed for 4 h. Cooled to ambient temperature, the reaction mixture was purified by preparative HPLC to afford the titled compound as solid (0.0030 g, y. 4%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08742113B2
Source datasetuspto-grants-2014_06
ORD IDord-5d311e557208471ebc544a6080e2ccf5
Source noteuspto-grants-2014_06