HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 402747Generated: October 31, 2026
Hydrazine hydrate (1:1) → HCID 178438829, compound
https://huagongshe.com/reaction/402747
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | dibenzyl 3-(2,3-dihydro-1H-inden-5-yl)-6-isopropyl-2-oxo-4-thioxo-3,4-dihydro-2H-benzo[e][1,3]oxazin-7-yl phosphate | HCID 86762470 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178438829 | HCID 178438829 | 31.1% |
Reaction Steps
To a stirred solution of 0.52 g (0.84 mmols) of 7 in 15 mL of anhydrous ethanol was added 63 mg (1.27 mmols) of hydrazine hydrate and the mixture stirred at 80° C. for 30 min. The mixture was concentrated and chromatographed on silica gel using 1:1 hexane:ethylacetate to afford 0.16 g of the product 8 as off-white foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08742133B2 |
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| Source dataset | uspto-grants-2014_06 |
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| ORD ID | ord-b698c4c7a3534d83be105b9145da7c19 |
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| Source note | uspto-grants-2014_06 |
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