HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 402756Generated: October 25, 2026
Potassium Carbonate → HCID 66765091, compound
https://huagongshe.com/reaction/402756
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Phenylhydrazine hydrochloride | HCID 60962 | — |
| Reactant | Ethyl 2,4,5-trifluorobenzoylacetate | HCID 2758933 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66765091 | HCID 66765091 | — |
Reaction Steps
Potassium carbonate (153 mg, 1.10 mmol) was added to a stirred mixture of phenyl hydrazine HCl salt (160 mg, 1.10 mmol) and ethyl 3-oxo-3-(2,4,5-trifluorophenyl)propanoate (272 mg, 1.10 mmol) in EtOH (6 mL) and the mixture was heated at 70° C. for 1 hour. The solution was cooled to room temperature and was concentrated to give the title compound, which was taken on to the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08742110B2 |
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| Source dataset | uspto-grants-2014_06 |
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| ORD ID | ord-3b8aeac09dcf44bfbc8b68645c6200f3 |
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| Source note | uspto-grants-2014_06 |
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