Hydrochloric Acid → HCID 66630655, compound

Participants

Reaction Steps

To a solution of N-cyclopropyl-4-methyl-3-({4-[(5-methylisoxazol-3-yl)methoxy]benzoyl}amino)benzamide (20 mg, 0.05 mmol) in 1:1 DCM and methanol (2.0 mL) was added hydrochloric acid (0.05 mmol). The solvent was evaporated to give the title compound; NMR Spectrum: (DMSOd6) 0.57 (m, 2H), 0.68 (m, 2H), 2.26 (s, 3H), 2.44 (s, 3H), 2.85 (m, 1H), 5.25 (s, 2H), 6.37 (s, 1H), 7.15 (m, 2H), 7.31 (m, 1H), 7.61 (m, 1H), 7.78 (s, 1H), 7.98 (m, 2H), 8.37 (s, 1H), 9.82 (s, 1H); Mass Spectrum: M−H− 404, M+Na+ 428.

Provenance & Evidence