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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 403063Generated: October 30, 2026

Hydrogen Bromide → HCID 66631091, compound

https://huagongshe.com/reaction/403063

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrogen BromideHCID 260—
ReactantHCID 11441018HCID 11441018—
ProductHCID 66631091HCID 66631091—

Reaction Steps

Using an analogous procedure to that described in Example 36, N-{5-[(cyclopropylamino)carbonyl]-2-methylphenyl}-5-(pyridin-2-ylmethoxy)pyridine-2-carboxamide was reacted with hydrobromic acid to give the title compound; NMR Spectrum: (DMSOd6) 0.58 (m, 2H), 0.69 (m, 2H), 2.32 (s, 3H), 2.86 (m, 1H), 5.49 (s, 2H), 7.33 (m, 1H), 7.58 (m, 1H), 7.76 (m, 2H), 7.95 (m, 1H), 8.15 (m, 2H), 8.34 (m, 2H), 8.53 (m, 1H), 8.82 (m, 1H), 10.13 (s, 1H); Mass Spectrum: M+H+ 403.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08742124B2
Source datasetuspto-grants-2014_06
ORD IDord-db081d00d687451ca8b21e84996e6121
Source noteuspto-grants-2014_06