Dimethyl Carbonate → HCID 23116056, compound

HRID 403077Notes

Reaction equation

HRID 403077 reaction equation
[CH3:1][O:2][CH2:3][N:4]1[CH2:8][CH2:7][CH2:6][CH2:5]1.[C:9](=[O:14])([O:12]C)[O:10][CH3:11]>>[CH3:11][O:10][C:9](=[O:12])[O-:14].[CH3:1][O:2][CH2:3][N+:4]1([CH3:9])[CH2:8][CH2:7][CH2:6][CH2:5]1

Participants

3

Reactant 2

HCID 12021Dimethyl CarbonateHCID 11412363HCID 11412363, compound

Product 1

HCID 23116056HCID 23116056, compoundYield 60%

Procedure

Methoxymethylpyrrolidine (10.00 g) and 117.39 g of dimethyl carbonate were placed into an autoclave and reacted at 120° C. for 24 hours. The resulting solids were filtered off and washed with dimethyl carbonate. The solids were dried in a vacuum, giving 10.70 g of the desired product.

Workup

  1. customreacted at 120° C. for 24 hours
  2. filtrationThe resulting solids were filtered off
  3. washwashed with dimethyl carbonate
  4. customThe solids were dried in a vacuum

Sources & evidence

ORD record
ord-9a8d7522c8874e3bb3685b1d19400e9a
Source dataset
uspto-grants-2014_06
Patent number
US08747690B2

Reaction notes

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