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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 403464생성일: 2026년 10월 25일

Potassium Carbonate → tert-Butyl [2,6-dimethyl-4-(5-methylsulfanyl-7-propoxyoxazolo[5,4-d]pyrimidin-2-yl)-phenoxy]acetate

https://huagongshe.com/reaction/403464

반응식

참여 물질

역할이름HCID투입량
반응물Potassium CarbonateHCID 11430—
반응물tert-Butyl bromoacetateHCID 79177—
반응물HCID 136389866HCID 136389866—
용매DimethylformamideHCID 6228—
생성물tert-Butyl [2,6-dimethyl-4-(5-methylsulfanyl-7-propoxyoxazolo[5,4-d]pyrimidin-2-yl)-phenoxy]acetateHCID 86688232—

반응 단계

To a solution of 2.00 g of 2,6-dimethyl-4-(5-methylsulfanyl-7-propoxy-oxazolo[5,4-d]pyrimidin-2-yl)-phenol in 20 ml of N,N-dimethylformamide was added 3.20 g of potassium carbonate, followed by 0.93 ml of tert-butyl bromoacetate. The mixture was reacted for 1 h at 60° C., then allowed to cool and poured onto water. The resulting precipitate was collected by filtration with suction and dried in vacuo. 2.45 g of the title compound were obtained.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08748436B2
출처 데이터셋uspto-grants-2014_06
ORD IDord-e07604bbafa143479c58699c0b130c21
출처 메모uspto-grants-2014_06