Phenyl isocyanate → HCID 66700186, compound

HRID 403675Notes

Reaction equation

HRID 403675 reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([CH:9]=[C:10]([I:14])[C:11]=1[O:12][CH3:13])[NH2:8])([CH3:4])([CH3:3])[CH3:2].[C:15]1([N:21]=[C:22]=[O:23])[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[C:1]([C:5]1[CH:6]=[C:7]([NH:8][C:22]([NH:21][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[O:23])[CH:9]=[C:10]([I:14])[C:11]=1[O:12][CH3:13])([CH3:4])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 7672Phenyl isocyanateHCID 57419443HCID 57419443, compound

Product 1

HCID 66700186HCID 66700186, compound

Procedure

3-tert-Butyl-5-iodo-4-methoxyaniline (305 mg, 1 mmol) and phenyl isocyanate (0.109 mL, 1.000 mmol) were reacted in the same manner as Example 15 Part A to give the title compound.

Sources & evidence

ORD record
ord-9e10f9ce3b304f45be7e78fa1a76a1ab
Source dataset
uspto-grants-2014_06
Patent number
US08748443B2

Reaction notes

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