Chlorophenyl isocyanate → HCID 67305795, compound

Participants

Reaction Steps

The compound of example 665 (100 mg. 0.284 mmol) was dissolved in tetrahydrofuran (10 mL) and to this solution, 2-chloro phenylisocyanate (65 mg. 0.426 mmol) was added. The reaction mixture was stirred at room temperature for 24 h. The solvent was removed completely to obtain a residue which was purified by column chromatography (silicagel, 30% ethyl acetate in chloroform) to afford the title compound.

Provenance & Evidence