HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → N-Hydroxy-4-(3-phenethyl-ureido)-butyramide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | 4-[3-(4-Dimethylamino-benzyl)-ureido]-N-hydroxy-butyramide | HCID 57598161 | — |
| Product | N-Hydroxy-4-(3-phenethyl-ureido)-butyramide | HCID 11334591 | — |
Reaction Steps
Compound 1 was prepared using the methodology described for the preparation of compound 2, by substituting 4-dimethylaminobenzylamine dihydrochloride with phenethylamine. 1H NMR (CD3OD) δ 7.30-7.15 (m, 5H), 3.34 (t, J=6.9 Hz, 2H), 3.11 (t, J=7.2 Hz, 2H), 2.76 (t, J=7.2 Hz, 2H), 2.09 (t, J=7.5 Hz, 2H), 1.73 (m, 2H). 13C NMR (CD3OD) δ 172.7, 161.3, 140.9, 130.0, 129.6, 127.4, 42.8, 40.4, 37.7, 31.3, 27.8.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08748463B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-cbaa9b8cd7ba474d8ea946e5c2f33750 |
| Source note | uspto-grants-2014_06 |