HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxide → Diphenyldiethylphosphonium hydroxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxide | HCID 961 | — |
| Reactant | Phosphonium, diethyldiphenyl-, iodide | HCID 357429 | — |
| Solvent | Water | HCID 962 | — |
| Product | Diphenyldiethylphosphonium hydroxide | HCID 18407746 | 96% |
Reaction Steps
This 98.45 g of diphenyldiethylphosphonium iodide was then dissolved in water, and converted to the corresponding hydroxide with 270 g of an anionic exchange resin in batch overnight, yielding 271.75 g of a 0.94 M solution of diphenyldiethylphosphonium hydroxide (96% of exchange yield) The diphenyldiethylphosphonium hydroxide was used as SDA source.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08529868B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-2249a546e80243079730b7f18d3febb6 |
| Source note | uspto-grants-2013_09 |