HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonic acid, 4-methyl-, compd. with pyridine (1:1) → HCID 58380014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonic acid, 4-methyl-, compd. with pyridine (1:1) | HCID 466102 | — |
| Reactant | HCID 58380306 | HCID 58380306 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58380014 | HCID 58380014 | 96% |
Reaction Steps
To a solution of 21.7 (100 mg, 234 μmol) in MeOH, was added PPTS (12 mg, 47 μmol). The resulting mixture was stirred overnight. Solvent was then removed in vacuo to give a residue which was purified by CombiFlash® chromatography to give the product as an oil (70 mg, 96%). MS ESI m/e: 330.2 (M+18)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08748462B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-12950b3ddf6143a6807d03598c365ca1 |
| Source note | uspto-grants-2014_06 |