Thionyl Chloride → HCID 57467660, compound

Participants

Reaction Steps

To a solution of (4-(5-fluoro-2-methoxypyridin-4-yl)-3-(1-(methoxymethyl)cyclopentyl)phenyl)methanol (71.0 mg, 206 μmol) DMF (10 uL), and DCM (4.0 mL) was slowly added thionyl chloride (15.0 μL, 206 μmol) at 0° C. After addition, the resulting mixture was stirred at room temperature for 1 hour. The solvent was removed providing the product which was used in the next step. MS ESI (pos.) m/e: 364.2 (M+H)+.

Provenance & Evidence