HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-1-chloro-isoquinoline → 6-Bromo-1,7-dichloroisoquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-1-chloro-isoquinoline | HCID 22250244 | — |
| Reactant | 6-Bromo-7-chloro-isoquinoline 2-oxide | HCID 59226262 | — |
| Product | 6-Bromo-1,7-dichloroisoquinoline | HCID 59226269 | — |
Reaction Steps
Starting with 6-Bromo-7-chloro-isoquinoline 2-oxide (10), the desired 6-Bromo-1,7-dichloro-isoquinoline was prepared by the method, described for 6-Bromo-1-chloro-isoquinoline (5). Rt=1.85 min (Method C). Detected mass: 276.1/278.2 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08748614B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-660c868533574e8990fc2e46687612ed |
| Source note | uspto-grants-2014_06 |