HRID40581

反应详情

EQUATION

反应方程式

HRID 40581 的结构方程式

CONDITIONS

反应条件

温度
80 °C

PROCEDURE

实验过程

A suspension of 6-chloro-2-methyl-quinoline (355 mg) and SeO2 (233 mg) in 1,4-dioxane (3 mL) was heated at 80° C. for 16 h. The resulting black mixture was filtered through diatomaceous earth. Concentration of the filtrate gave the title compound as a yellow powder (324 mg).

WORKUP

后处理

  1. filtrationThe resulting black mixture was filtered through diatomaceous earth