HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxyphenol → 4-Methoxycyclohexanol (cis,trans)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Methoxycyclohexanol (cis,trans) | HCID 140332 | — |
Reaction Steps
4-Methoxyphenol (100 g) in ethanol (759 ml) was hydrogenated under 50 psi hydrogen using Nishimura catalyst (10.0 g) at rt for 4.5 h. The catalyst was filtered off; the solvent was removed in vacuo to yield the desired product as 95% pure yellowish liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08754079B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-66c84cbcff4b405b833f38f35bbb2adf |
| Source note | uspto-grants-2014_06 |