5-Fluoro-2-nitrophenol → HCID 58421507, compound

HRID 406037Notes

Reaction equation

HRID 406037 reaction equation
[C:1]1([OH:6])[CH2:5][CH2:4][CH2:3][CH:2]=1.[F:7][C:8]1[CH:9]=[CH:10][C:11]([N+:15]([O-:17])=[O:16])=[C:12](O)[CH:13]=1.CCOC(/N=N/C(OCC)=O)=O>>[CH:1]1([O:6][C:10]2[CH:9]=[C:8]([F:7])[CH:13]=[CH:12][C:11]=2[N+:15]([O-:17])=[O:16])[CH2:5][CH:4]=[CH:3][CH2:2]1

Participants

4

Reactant 3

HCID 99375-Fluoro-2-nitrophenolHCID 18569CyclopentenolHCID 5462977Diethyl azodicarboxylate

Product 1

HCID 58421507HCID 58421507, compound

Procedure

Prepared analogously to XVI.1 from 1 g cyclopentenol, 1.57 g 5-fluoro-2-nitro-phenol and 1.89 ml DEAD.

Sources & evidence

ORD record
ord-2ec51effd80f41918983622aeb6bdc3a
Source dataset
uspto-grants-2014_06
Patent number
US08754079B2

Reaction notes

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